CIA Reading Room cia rdp86 00513r000927930007 4 pdf

CIA Reading Room cia rdp86 00513r000927930007 4

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L; 1″) 8 ,/ 6 2 /0 0 0/ C) Ir all or) III fur … ()/’0,: 5,/Of the decornponition proceasen.transiation.i Ab3tracter’o note:Car.’ 2125/013 62/000/005/040/1″2B1 51XB101AUTPORSt Titz-5kvort3ova, 1. 11. , ‘-“‘ ybnikova, A. A., Kuvshinova, N. N.TITLF.; Tran.-formation of -decylthiophane in the pre3ence of analuminosilicate catalystP,–,aiODICALs Referativnyy zhurnal. Khimiya, no. 5, 1962, 264, abstract5Zh238 (5b. “Yhimiya seraorgan. zoyedineniy,soderzhashchikhoya v neftyakh i nefteproduktakh. v. 4”.M., Gostoptekhizdat, 1961, 136-140)TEXT: The reaction between furfural and C 9H19 MpBr is used to obtain-nonylfurylcarbinol M (here and later the calculated yields in 4Zo I L,@b. P. in OC/mm Hg, m. p. in 0C, n20 D and d420 )t 76, 144-145/5, 5.991-46065, 0.9326; by the action of HCl and C 2H5OH I i:j converted to “heethyl ester of -keto-tetradecanic acid (11), )5, 142-144/3, 17, 1.4508,0.9227; by the reduction of II with LiAlH 4totradecandiol-1,4 (111) isCard 1/23/081/62/000/00ri/040/112Transformation of –deuylthiophane … B151/B101obtainedi 73-98, 172-174/5, 57.3, -, -; by the reduction with HBr gas IIIis convurted to 1,4-dibromo-tetradecane (IV), 70, 18?-18419, -, 1.4857,1.2174; by the reaction of IV wLth Na 2S,.-decylthiophane (V) 13 obtaine-di75-80, 140.5-149/5-5, -, 1.4804, 0-6959; the complex Yith 11gC1 2 has aM.

P. 47-50C. The contact conversion of V on an aluminosilicate cataljst(ASC) is studied. V is passed witi, a volume rate of 0.5 hro- 1 over AN(73-314V ASC or. the vt. of V) in a stream of ‘1112at .11000C.H25 is obtainedin a yield of 53-7@6 (on the 3 content in V) and tetradecene-1, C 14H289b. p. 80-820//8 mm Hg, n20D 1-4383, d 20 0.7841. @Abstracti@rls note_4Co=olete translation.Card 212TITS-Sh-VORTSOVA, I.N.; RYBNIKOVA, A.A. j KUMITNOVA,- -Synthesis and cataly-tic conversion.,j of v

• Creator/s: CIA Reading Room
• Date: 12/31/1967
• Book Topics/Themes: CIA Reading Room

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